workshops:epma_masterclass

EPMA Masterclass

Workshop description

The EPMA Masterclass is a full-day workshop focussed on cutting-edge techniques and applications in EPMA microanalysis, mapping, and spectroscopy. This masterclass includes the cryogenic EPMA workshop in the morning session, and the advanced EPMA workshop in the afternoon session.

This Masterclass is kindly sponsored by Microscopy Australia.

Morning session: Cryogenic EPMA

Topics covered in this workshop include:

  • Introduction to sample preparation requirements for cold stage, including the need for thin metal coats which are mechanically able to withstand the stress of being cooled and any changes in sample while cooling.
  • Introduction to how cryo-cooled specimen stages use cool nitrogen gas, in preference to liquid nitrogen, to reduce mechanical vibration and to decouple from the cryogenic liquid supply. The discussion will include cryo-stage design to minimise mechanical drift.
  • Discussion on minimising ice formation on the cryogenically cooled sample surface, including best practices and strategies to remove ice.
  • Theory and practice of cryo-microanalysis or the analysis of minerals with high water content. These minerals cannot have accurate microanalysis performed at room temperature. Many secondary highly hydrated minerals suffer for beam instability at room temperature.
  • Demonstration of cryo-CL imaging where we see 5-10 times increases in cathodoluminescence emission due to the removal of thermal robbing processes.

Please refer to the Cryo EPMA workshop page for more information about this session of the EPMA Masterclass.

Afternoon session: Advanced EPMA

This half day workshop will focus upon the theory and practice of advanced electron probe microanalysis techniques, covering key topics like CL, trace element analysis, and peak overlap corrections for Rare Earth microanalysis. It will provide a review of advanced techniques for more experienced users. The emphasis will be on analysis of inorganic polished samples, with discussion to include thin films, and other materials as they are brought up by the attendees.

Topics will include:

  • Different stages available in the EPMA
  • Rare earth element analysis
  • Selection and sourcing of microanalysis standards
  • Multi-voltage analysis
  • Mass absorption coefficient tables
  • Trace element mapping
  • Compositional mapping and cluster analysis
  • EDS peak extraction
  • CL mapping and quantitative calibration by EPMA or LA-ICPMS
  • Cryo-microanalysis

Please refer to the Advanced EPMA workshop page for more information about this session of the EPMA Masterclass.

Date and time

The workshop will be held on Monday the 9th of February, starting at 9:00am.

Location

The workshop will be held at CSIRO Mineral Resources, in Clayton.

Attendees of this EPMA Masterclass may also be interested in attending one or more of the related workshops on Tuesday, including:

Monday workshops

Workshop Time Location / directions
Laser Ablation User Group Meeting and Workshop 9am-5pm Ian Wark Theatre, Central Precinct, CSIRO Clayton Site, Research Way, Clayton. Go to CSIRO Central reception.
Electron Backscatter Diffraction 9am-5pm Seminar Room 4.07 and 4.08, New Horizons building, 20 Research Way, Clayton Campus, Monash University. Go to the New Horizons Building.
Focused Ion Beam 9am-5pm Reid Room, Level 1, Bld 125, Western Precinct, CSIRO Clayton Site, Research Way, Clayton. Go to CSIRO Western reception.
Fundamentals of EPMA 9am-12:30pm Clive Pratt Room, Bld 121, Western Precinct, CSIRO Clayton Site, Research Way, Clayton. Go to CSIRO Western reception.
Cryogenic EPMA (EPMA Masterclass) 9am-12:30pm GK Williams Room, Bld 121, Western Precinct, CSIRO Clayton Site, Research Way, Clayton. Go to CSIRO Western reception.
Advanced EPMA (EPMA Masterclass) 1:30pm-5:00pm GK Williams Room, Bld 121, Western Precinct, CSIRO Clayton Site, Research Way, Clayton. Go to CSIRO Western reception.

Tuesday workshops

Workshop Time Location / directions
Art and Cultural Heritage: Conservation, Microscopy and Analysis 9:00am-4:30pm National Gallery of Victoria, ​180 St Kilda Road, Melbourne.
Advanced Specimen Preparation for Microanalysis 9:00am-5pm EL Archer Room (morning), Level 1, Bld 121, Western Precinct, CSIRO Clayton Site, Research Way, Clayton. Go to CSIRO Western reception. Afternoon: Laboratories, Blds 125/126.
Soft X-ray Spectroscopy Collection and Analysis 9:00am-5pm Clive Pratt Room, Bld 121, Western Precinct, CSIRO Clayton Site, Research Way, Clayton. Go to CSIRO Western reception.
Automated Mineralogy 9:00am-12:30pm GK Williams Room, Bld 121, Western Precinct, CSIRO Clayton Site, Research Way, Clayton. Go to CSIRO Western reception.
Monte Carlo Modelling 1:30pm-5pm EL Archer Room, Level 1, Bld 121, Western Precinct, CSIRO Clayton Site, Research Way, Clayton. Go to CSIRO Western reception.

For the full list of workshops, please refer to the workshop program page.

Registration

Masterclass sponsor

This Masterclass is kindly sponsored by Microscopy Australia.
Last modified: 2025/11/27 14:36